3-Nitro-N-(pyridin-4-yl)pyridin-2-amine → HCID 12445535, 화합물

HRID 1974324노트

반응식

HRID 1974324 반응식
[N+:1]([C:4]1[C:5]([NH:10][C:11]2[CH:16]=[CH:15][N:14]=[CH:13][CH:12]=2)=[N:6][CH:7]=[CH:8][CH:9]=1)([O-])=O>[Pd].CO>[NH2:1][C:4]1[C:5]([NH:10][C:11]2[CH:16]=[CH:15][N:14]=[CH:13][CH:12]=2)=[N:6][CH:7]=[CH:8][CH:9]=1

참가 물질

4

반응물 1

HCID 124453923-Nitro-N-(pyridin-4-yl)pyridin-2-amine

생성물 1

HCID 12445535HCID 12445535, 화합물

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 887Methanol용매

실험 절차

The nitro compound from Step A (1.0 g.) was hydrogenated in 60 ml. of methanol over 0.2 g. of 5% palladium on carbon catalyst. The catalyst was removed by filtration and the filtrate was evaporated to dryness.

후처리

  1. customThe catalyst was removed by filtration
  2. customthe filtrate was evaporated to dryness

출처 및 근거

ORD 기록
ord-ea124cf1a6c54326bf7e664de0c6bc0c
출처 데이터셋
uspto-grants-1976_12
특허 번호
US04000286

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