Dl-Tryptophan → 39545-27-2

HRID 1974341노트

반응식

HRID 1974341 반응식
[Cl:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4](Cl)=[O:5].[NH2:11][CH:12]([C:23]([OH:25])=[O:24])[CH2:13][C:14]1[C:22]2[C:17](=[CH:18][CH:19]=[CH:20][CH:21]=2)[NH:16][CH:15]=1>>[Cl:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([NH:11][CH:12]([C:23]([OH:25])=[O:24])[CH2:13][C:14]1[C:22]2[C:17](=[CH:18][CH:19]=[CH:20][CH:21]=2)[NH:16][CH:15]=1)=[O:5]

참가 물질

3

반응물 2

HCID 1148Dl-TryptophanHCID 691102-Chlorobenzoyl chloride

생성물 1

HCID 373257539545-27-2수율 84%

실험 절차

The same procedure is used as in Example 1, o-chlorobenzoyl chloride and DL-tryptophane being used. Yield 84%. Melting point 56° to 70° C.

출처 및 근거

ORD 기록
ord-2f342c9fa42d45d58b4d41fc180aedd6
출처 데이터셋
uspto-grants-1976_12
특허 번호
US04000297

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