Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chloroform → HCID 18766188, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chloroform | HCID 6212 | — |
| 반응물 | n-Heptyl isocyanate | HCID 138341 | — |
| 반응물 | 1-(Aminooxy)-3-(piperidin-1-yl)propan-2-ol | HCID 18766210 | — |
| 생성물 | HCID 18766188 | HCID 18766188 | — |
반응 단계
To the solution of 1.23 g (7.1 mmol) of l-aminooxy-2-hydroxy-3-(1-piperidinyl)-propane dissolved in 20 ml of chloroform 1.0 g (7.1 mmol) of heptyl isocyanate was added and the reaction mixture was stirred for 20 hours. Solvent was evaporated in vacuum and the residue was purified by chromatography to give pure colorless oil. White crystalline product was obtained by triturating with petroleum ether.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07745465B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-5d41a87368eb46de9294345e9b841d10 |
| 출처 메모 | uspto-grants-2010_06 |