Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
6-Bromohexanamide → 4-[7-(1-Adamantyl)-6-carbamoylpentyloxy-2-naphthyl]benzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 6-Bromohexanamide | HCID 321974 | — |
| 반응물 | Methyl 4-[7-(1-adamantyl)-6-hydroxy-2-naphthyl]benzoate | HCID 22000367 | — |
| 생성물 | 4-[7-(1-Adamantyl)-6-carbamoylpentyloxy-2-naphthyl]benzoic acid | HCID 70230932 | 65.6% |
반응 단계
Following the procedure of Example 12(a), but reacting 640 mg (1.55 mmol) of methyl 4-[7-(1-adamantyl)-6-hydroxy-2-naphthyl]benzoate with 450 mg (2.32 mmol) of 6-bromohexanamide, 520 mg (65%) of the expected compound were obtained, which compound had a melting point of 209°-10° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06225328B1 |
| 출처 데이터셋 | uspto-grants-2001_05 |
| ORD ID | ord-530f64406b1d4ee588c744046266f245 |
| 출처 메모 | uspto-grants-2001_05 |