Water → 4-N,N-dimethylaminophenylacetic acid

HRID 1976760

반응식

[CH3:1][N:2]([CH2:4][CH2:5][CH2:6]C(=C)C(N)=O)[CH3:3].CCl.[C:14](N)(=[O:17])[CH:15]=[CH2:16].N([C:27]([CH3:32])(C)C(N)=N)=NC(C)(C)C(N)=N.[OH2:33]>>[CH3:3][N:2]([C:4]1[CH:5]=[CH:6][C:16]([CH2:15][C:14]([OH:17])=[O:33])=[CH:32][CH:27]=1)[CH3:1]

참가 물질

반응물 5

HCID 962Water

HCID 19692,2'-Diazenediylbis(2-methylpropanimidamide)

HCID 6327Methyl Chloride

HCID 6579Acrylamide

HCID 18359659Dimethylaminopropylacrylamide

생성물 1

HCID 1522034-N,N-dimethylaminophenylacetic acid

실험 절차

CH3CL/dimethylaminopropylacrylamide, quaternized with methyl chloride, and 29 g of acrylamide were added to 541 g of water with 200 mg azo-bisisobutyroamidine (AIBA) and after passage of nitrogen therethrough, the mixture was irradiated for 30 minutes by an Osram HWL 250-W lamp. The gel so obtained was dried to a residual water content of 9% and ground.

후처리

customThe gel so obtained
dry with materialwas dried to a residual water content of 9% and ground

출처 및 근거

ORD 기록: ord-b975593d5010421ea0038864bc29a1c2
출처 데이터셋: uspto-grants-2001_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06228964B1

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