Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Cyclohexanol → 5-Methyloxepan-2-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Cyclohexanol | HCID 7966 | — |
| 반응물 | Cyclohexanone | HCID 7967 | — |
| 반응물 | 4-Methylcyclohexanol | HCID 11524 | — |
| 반응물 | 4-Methylcyclohexanone | HCID 11525 | — |
| 생성물 | 5-Methyloxepan-2-one | HCID 11116085 | 45.6% |
반응 단계
The procedure of Example 25 was repeated, except that 4-methylcyclohexanone (2 mmol) and 4-methylcyclohexanol (20 mmol) were respectively used in stead of cyclohexanone and cyclohexanol. As a result, γ-methyl-ε-caprolactone was formed in yield of 45.6% (on 4-methylcyclohexanone basis).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06229023B1 |
| 출처 데이터셋 | uspto-grants-2001_05 |
| ORD ID | ord-e9be06758656493f86556ad392cedec9 |
| 출처 메모 | uspto-grants-2001_05 |