Mls000756500 → 3-Amino-N-3-pyridinylbenzamide
반응식
[N+:1]([C:4]1[CH:5]=[C:6]([CH:16]=[CH:17][CH:18]=1)[C:7]([NH:9][C:10]1[CH:11]=[N:12][CH:13]=[CH:14][CH:15]=1)=[O:8])([O-])=O>C(O)C.[Pd]>[NH2:1][C:4]1[CH:5]=[C:6]([CH:16]=[CH:17][CH:18]=1)[C:7]([NH:9][C:10]1[CH:11]=[N:12][CH:13]=[CH:14][CH:15]=1)=[O:8]참가 물질
4
실험 절차
A solution of 3-(3-nitrobenzoylamino)-pyridine (2 g, 8.23 mmol) in ethanol (200 ml) was treated with 10% palladium on charcoal (0.5 g) and hydrogenated at atmospheric pressure for 4 h. Filtration and evaporation afforded the product as a white solid (1.51 g, 86%).
후처리
- filtrationFiltration and evaporation
출처 및 근거
- ORD 기록
- ord-dda6ea9e01e443e2a2bf3670799ac9e3
- 출처 데이터셋
- uspto-grants-2001_05
- 특허 번호
- US06235758B1
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