Flamenol → HCID 17871222, 화합물

HRID 1977957노트

반응식

HRID 1977957 반응식
[CH3:1][S:2]([C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=1[S:11](Cl)(=[O:13])=[O:12])(=[O:4])=[O:3].[CH3:15][O:16][C:17]1[CH:18]=[C:19]([OH:24])[CH:20]=[C:21]([CH:23]=1)[OH:22]>>[CH3:15][O:16][C:17]1[CH:23]=[C:21]([O:22][S:11]([C:6]2[CH:7]=[CH:8][CH:9]=[CH:10][C:5]=2[S:2]([CH3:1])(=[O:4])=[O:3])(=[O:13])=[O:12])[CH:20]=[C:19]([OH:24])[CH:18]=1

참가 물질

3

반응물 2

HCID 71648FlamenolHCID 27351782-Methanesulfonylbenzene-1-sulfonyl chloride

생성물 1

HCID 17871222HCID 17871222, 화합물수율 80%

실험 절차

The title compound was prepared in 80% yield from 2-methylsulfonylbenzenesulfonyl chloride and 5-methoxyresorcinol in a manner analogous to step a of Example 1. 1H-NMR (300 MHz, CDCl3) δ8.42 (d, J=7.8 Hz, 1H), 8.13 (d, J=7.8 Hz, 1H), 7.88 (t, J=7.8 Hz, 1H), 7.75 (t, J=7.7 Hz, 1H), 6.36 (s, 1H), 6.31 (s, 1H), 6.28 (s, 1H), 3.68 (s, 3H), 3.45 (s, 3H).

출처 및 근거

ORD 기록
ord-039ee1a4e8784a05b498e38fa56486ab
출처 데이터셋
uspto-grants-2001_05
특허 번호
US06235778B1

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