1,3-Dicarboxy-5,7-adamantanediol → 1,3-Dicarboxy-5-acryloyloxy-7-adamantanol

HRID 1978117

반응식

HRID 1978117 반응식
[C:1](OCC12CC3CC(CC(O)(C3)C1)C2)(=[O:4])[CH:2]=[CH2:3].[C:18]([C:21]12[CH2:31][C:25]3([OH:32])[CH2:26][C:27]([OH:30])([CH2:29][C:23]([C:33]([OH:35])=[O:34])([CH2:24]3)[CH2:22]1)[CH2:28]2)([OH:20])=[O:19]>>[C:33]([C:23]12[CH2:24][C:25]3([O:32][C:1](=[O:4])[CH:2]=[CH2:3])[CH2:26][C:27]([OH:30])([CH2:28][C:21]([C:18]([OH:20])=[O:19])([CH2:31]3)[CH2:22]1)[CH2:29]2)([OH:35])=[O:34]

참가 물질

3

반응물 2

HCID 120704631,3-Dicarboxy-5,7-adamantanediolHCID 219967831-Hydroxy-3-(acryloyloxymethyl)adamantane

생성물 1

HCID 219967981,3-Dicarboxy-5-acryloyloxy-7-adamantanol수율 86%

실험 절차

The reaction was conducted in the same manner as said (2) except that 1,3-dicarboxy-5,7-dihydroxyadamantane was used instead of the 1,3-dicarboxy-5-adamantanol, and, as a result, a 1,3-dicarboxy-5-acryloyloxy-7-adamantanol (yield: 86%, white solid) was obtained.

출처 및 근거

ORD 기록
ord-6ffc86460638473fa3e06d4d28bbea4c
출처 데이터셋
uspto-grants-2001_05
특허 번호
US06235851B1

연결된 노트

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