1-Acetyl-3-hydroxyadamantane → 1-Acety-3-acryloyloxyadamantane

HRID 1978121

반응식

HRID 1978121 반응식
[C:1](OCC12CC3CC(CC(O)(C3)C1)C2)(=[O:4])[CH:2]=[CH2:3].[C:18]([C:21]12[CH2:30][CH:25]3[CH2:26][CH:27]([CH2:29][C:23]([OH:31])([CH2:24]3)[CH2:22]1)[CH2:28]2)(=[O:20])[CH3:19]>>[C:18]([C:21]12[CH2:30][CH:25]3[CH2:26][CH:27]([CH2:29][C:23]([O:31][C:1](=[O:4])[CH:2]=[CH2:3])([CH2:24]3)[CH2:22]1)[CH2:28]2)(=[O:20])[CH3:19]

참가 물질

3

반응물 2

HCID 5918961-Acetyl-3-hydroxyadamantaneHCID 219967831-Hydroxy-3-(acryloyloxymethyl)adamantane

생성물 1

HCID 698242441-Acety-3-acryloyloxyadamantane수율 97%

실험 절차

The reaction was conducted in the same manner as the step of Example 36 (2) except that 1-acetyl-3-hydroxyadamantane was used instead of the 1,3-dicarboxy-5-adamantanol, and, as a result, a 1-acety-3-acryloyloxyadamantane (yield: 97%, white solid) was obtained.

출처 및 근거

ORD 기록
ord-657d8ec62c2b4760a72e8a5e0b9fb64d
출처 데이터셋
uspto-grants-2001_05
특허 번호
US06235851B1

연결된 노트

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