Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Furfuryl Alcohol → Bis[(furan-2-yl)methyl] pentanedioate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Furfuryl Alcohol | HCID 7361 | — |
| 반응물 | Dimethyl Glutarate | HCID 14242 | — |
| 반응물 | Sodium | HCID 5360545 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Bis[(furan-2-yl)methyl] pentanedioate | HCID 20274632 | — |
반응 단계
196 parts by wt. of furfuryl alcohol and 160 parts by wt. dimethyl glutarate (stoichiometric proportions) were mixed and 0.5-0.75% wt. sodium metal added. The mixture was heated to a temperature in the range from 214°-240° F. under a nitrogen atmoshpere. Methanol was evolved and removed as the reaction progressed. After a period of 4 hours, a waxy solid was obtained. After washing the product with water, the residure was a liquid which was identified as difurfuryl glutarate by gas chromatography and mass spectrometric analysis.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04481310 |
| 출처 데이터셋 | uspto-grants-1984_11 |
| ORD ID | ord-465899fe373e4d44abcf7f61f98ca88c |
| 출처 메모 | uspto-grants-1984_11 |