Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzyl 1-aminocyclopentane-1-carboxylate → HCID 13376657, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzyl 1-aminocyclopentane-1-carboxylate | HCID 231228 | — |
| 반응물 | 4-Methoxy-2-methyl-4-oxobutanoic acid | HCID 4563901 | — |
| 생성물 | HCID 13376657 | HCID 13376657 | — |
반응 단계
1-[(3-Methoxycarbonyl-2-methylpropanoyl)amino]-1-cyclopentanecarboxylic acid, benzyl ester was prepared as described in Example 3 from 10.96 g (0.050 mol) of 1-amino-1-cyclopentanecarboxylic acid, benzyl ester and 7.31 g (0.050 mol) of 3-methoxycarbonyl-2-methylpropionic acid. Crude di-ester crystallized to give 13.57 g (78%) of an off-white solid, mp: 88°-93°. This was used without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04482572 |
| 출처 데이터셋 | uspto-grants-1984_11 |
| ORD ID | ord-6e38844d57004eafbada95de2f3d7f27 |
| 출처 메모 | uspto-grants-1984_11 |