Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,2-Ethanediamine, N1,N1-bis(1-methylethyl)- → N-[2-[bis(1-Methylethyl)amino]ethyl]-3-(phenylsulfonyl)-1-piperidinecarboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,2-Ethanediamine, N1,N1-bis(1-methylethyl)- | HCID 8459 | — |
| 반응물 | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| 반응물 | 3-(Phenylsulfonyl)piperidine | HCID 13607983 | — |
| 생성물 | N-[2-[bis(1-Methylethyl)amino]ethyl]-3-(phenylsulfonyl)-1-piperidinecarboxamide | HCID 13608029 | 59.8% |
반응 단계
Following the procedure of Example 16, diisopropylaminoethylamine and 1,1'-carbonyldiimidazole and 3-(phenylsulfonyl)piperidine were reacted to give the title compound which was crystallized from diethyl ether-hexane as white solid in 59.8% yield, m.p. 82.5°-84° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04593102 |
| 출처 데이터셋 | uspto-grants-1986_06 |
| ORD ID | ord-90509a2c407944e5b8b6920bf2310138 |
| 출처 메모 | uspto-grants-1986_06 |