4-Chlorobenzyl alcohol → HCID 67528502, 화합물

HRID 1982895노트

반응식

HRID 1982895 반응식
Br[C:2]1[CH:3]=[N+:4]([O-])[CH:5]=[CH:6][C:7]=1[N+:8]([O-:10])=[O:9].[Cl:12][C:13]1[CH:20]=[CH:19][C:16]([CH2:17][OH:18])=[CH:15][CH:14]=1>>[Cl:12][C:13]1[CH:20]=[CH:19][C:16]([CH2:17][O:18][C:2]2[CH:3]=[N:4][CH:5]=[CH:6][C:7]=2[N+:8]([O-:10])=[O:9])=[CH:15][CH:14]=1

참가 물질

3

반응물 2

HCID 133974-Chlorobenzyl alcoholHCID 5485213-Bromo-4-nitropyridine N-oxide

생성물 1

HCID 67528502HCID 67528502, 화합물수율 25.3%

실험 절차

In accordance with the same procedures as in Steps 3 and 4 of Preparation 1, except for using 3-bromo-4-nitropyridin-N-oxide prepared in Step 2 of Preparation 1 and 4-chlorobenzyl alcohol, the titled compound was obtained as a white solid. (Yield: 25.3% )

후처리

  1. customIn accordance with the same procedures as in Steps 3 and 4 of Preparation 1

출처 및 근거

ORD 기록
ord-86b5a30fd46c45a98d878ac6ee20d232
출처 데이터셋
uspto-grants-2009_06
특허 번호
US07541366B2

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