Benzene, 1-chloro-3-isocyanato- → Dimethyl 2-[3-({[(3-chloroanilino)carbonyl]oxy}methyl)benzyl]malonate

HRID 1985345

반응식

HRID 1985345 반응식
[OH:1][CH2:2][C:3]1[CH:4]=[C:5]([CH:16]=[CH:17][CH:18]=1)[CH2:6][CH:7]([C:12]([O:14][CH3:15])=[O:13])[C:8]([O:10][CH3:11])=[O:9].[Cl:19][C:20]1[CH:21]=[C:22]([N:26]=[C:27]=[O:28])[CH:23]=[CH:24][CH:25]=1>>[Cl:19][C:20]1[CH:21]=[C:22]([CH:23]=[CH:24][CH:25]=1)[NH:26][C:27]([O:1][CH2:2][C:3]1[CH:4]=[C:5]([CH:16]=[CH:17][CH:18]=1)[CH2:6][CH:7]([C:8]([O:10][CH3:11])=[O:9])[C:12]([O:14][CH3:15])=[O:13])=[O:28]

참가 물질

3

반응물 2

HCID 17968Benzene, 1-chloro-3-isocyanato-HCID 22926882Dimethyl 2-[3-(hydroxymethyl)benzyl]malonate

생성물 1

HCID 57719967Dimethyl 2-[3-({[(3-chloroanilino)carbonyl]oxy}methyl)benzyl]malonate

실험 절차

Using dimethyl 2-[3-(hydroxymethyl)benzyl]malonate and 3-chlorophenylisocyanate, the title compound was obtained in the same manner as described in Example 192b).

출처 및 근거

ORD 기록
ord-abaa763aecc64fecad90cbd21e1b61e3
출처 데이터셋
uspto-grants-2009_06
특허 번호
US07544835B2

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