참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Ethyl Bromide | HCID 6332 | — |
| 반응물 | 1,3-Dibromopropane | HCID 8001 | — |
| 반응물 | Triethyl phosphite | HCID 31215 | — |
| 생성물 | Diethyl (3-bromopropyl)phosphonate | HCID 283500 | — |
반응 단계
A mixture of 605 g (3.0 mol) of 1,3-dibromopropane and 250 g (1.5 mol) of triethyl phosphite was heated at an oil bath temperature of 130° C., while stirring and passing in nitrogen, for approximately 5 hours until approximately 154 g (1.5 mol) of bromoethane distilled over into a strongly ice-cooled receiver. The reaction mixture was distilled first in a bulb tube and then fractionally.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05728686 |
|---|
| 출처 데이터셋 | uspto-grants-1998_03 |
|---|
| ORD ID | ord-0e2048f259f14c369c409d485f3d1e95 |
|---|
| 출처 메모 | uspto-grants-1998_03 |
|---|
