Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Isobutyl-1-methylxanthine → N7-bromoehtyl 3-isobutyl-1-methylxanthine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Isobutyl-1-methylxanthine | HCID 3758 | — |
| 반응물 | 2-Bromoethylamine | HCID 7851 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | N7-bromoehtyl 3-isobutyl-1-methylxanthine | HCID 69056164 | — |
반응 단계
The process of preparing the compound of formula I comprises the steps of dissolving 3-isobutyl-1-methylxanthine (IBMX) into methanol and stirring with 2-bromoethylamine upon a mantle heater, reacting this mixture with NaOH and then recrystallizing this mixture with methanol to obtain N7-bromoehtyl 3-isobutyl-1-methylxanthine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07550468B2 |
| 출처 데이터셋 | uspto-grants-2009_06 |
| ORD ID | ord-2844dad69a4b4a888264a6e4aab7ae9d |
| 출처 메모 | uspto-grants-2009_06 |