HCID 86613205, 화합물 → HCID 69075811, 화합물

반응식

[OH:1][C@@H:2]([CH2:18][CH2:19][CH2:20][CH3:21])[C@H:3]([NH:10]C(=O)OC(C)(C)C)[CH2:4][C:5]1[CH:9]=[CH:8][S:7][CH:6]=1.C([C@H](NC(=O)OC(C)(C)C)[C@@H](O)CCCC)C1C=CC=CC=1>>[NH2:10][C@@H:3]([C@@H:2]([OH:1])[CH2:18][CH2:19][CH2:20][CH3:21])[CH2:4][C:5]1[CH:9]=[CH:8][S:7][CH:6]=1

참가 물질

반응물 2

HCID 86613205HCID 86613205, 화합물

HCID 86613206tert-butyl (1S,2S)-1-benzyl-2-hydroxyhexylcarbamate

생성물 1

HCID 69075811HCID 69075811, 화합물

실험 절차

Prepared from the Boc removal of the anti diastereoisomer tert-butyl (1R,2S)-2-hydroxy-1-(thien-3-ylmethyl)hexylcarbamate using a similar procedure as described in intermediate I step D. ES MS (M+H)=214.

출처 및 근거

ORD 기록: ord-3ce45e09343742508c1dfc69a063c9c0
출처 데이터셋: uspto-grants-2009_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07550481B2

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