Allyl bromide → HCID 178456405, 화합물

HRID 1987508노트

반응식

[NH2:1][N:2]1[CH:6]=[CH:5][N:4]=[N:3]1.[CH2:7]([Br:10])[CH:8]=[CH2:9]>>[Br-:10].[NH2:1][N+:2]1[CH:6]=[CH:5][N:4]([CH2:9][CH:8]=[CH2:7])[N:3]=1

참가 물질

반응물 2

HCID 7841Allyl bromide

HCID 38257231H-1,2,3-Triazol-1-amine

생성물 1

HCID 178456405HCID 178456405, 화합물수율 75%

실험 절차

In the aforementioned method, 1-amino-1,2,3-triazole (2) 5.00 g (59.5 mmoles) was reacted with allyl bromide 35.00 g (289 mmoles) at 20° C., and upon work-up resulted in a yield of 9.03 g (75%) of 1-amino-3-(2-propenyl)-1,2,3-triazolium bromide (2d), mp 100-101° C.

출처 및 근거

ORD 기록: ord-78b29ebc09544a7b958fa682d7e221a4
출처 데이터셋: uspto-grants-2009_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07550601B1

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