4-Chlorobenzyl alcohol → 4-[(4-Chlorophenyl)methoxy]-3-nitropyridine

반응식

Cl[C:2]1[CH:7]=[CH:6][N:5]=[CH:4][C:3]=1[N+:8]([O-:10])=[O:9].[Cl:11][C:12]1[CH:19]=[CH:18][C:15]([CH2:16][OH:17])=[CH:14][CH:13]=1>>[Cl:11][C:12]1[CH:19]=[CH:18][C:15]([CH2:16][O:17][C:2]2[CH:7]=[CH:6][N:5]=[CH:4][C:3]=2[N+:8]([O-:10])=[O:9])=[CH:14][CH:13]=1

참가 물질

반응물 2

HCID 133974-Chlorobenzyl alcohol

HCID 27357814-Chloro-3-nitropyridine

생성물 1

HCID 687003244-[(4-Chlorophenyl)methoxy]-3-nitropyridine수율 78%

실험 절차

In accordance with the same procedures as in Preparation 2, except for using 4-chloro-3-nitropyridine prepared in Step 1 of Preparation 1 and 4-chlorobenzyl alcohol, the titled compound was obtained as a white solid. (Yield: 78.0%)

후처리

customIn accordance with the same procedures as in Preparation 2

출처 및 근거

ORD 기록: ord-0e2bd51a65b94b20b9d409262b107226
출처 데이터셋: uspto-grants-2010_01
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07642269B2

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