HCID 68522041, 화합물 → HCID 86612410, 화합물

HRID 1990084노트

반응식

HRID 1990084 반응식
COC(C1SC([N:22]=[N+:23]=[N-:24])=C(C#N)C=1C1C=CC=CC=1C(C)(C)C)=O.[CH2:25]([O:27][C:28]([C:30]1[S:31][C:32](S(C)(=O)=O)=[C:33]([C:42]#[N:43])[C:34]=1[C:35]1[CH:40]=[CH:39][C:38]([I:41])=[CH:37][CH:36]=1)=[O:29])[CH3:26]>>[CH2:25]([O:27][C:28]([C:30]1[S:31][C:32]([N:22]=[N+:23]=[N-:24])=[C:33]([C:42]#[N:43])[C:34]=1[C:35]1[CH:40]=[CH:39][C:38]([I:41])=[CH:37][CH:36]=1)=[O:29])[CH3:26]

참가 물질

3

반응물 2

HCID 68522041HCID 68522041, 화합물HCID 86612409HCID 86612409, 화합물

생성물 1

HCID 86612410HCID 86612410, 화합물

실험 절차

Using a method substantially in accordance with the method of example 5-azido-3-(tert-butyl-phenyl)-4-cyano-thiophene-2-carboxylic acid methyl ester starting with the compound 3-(4-iodophenyl)-4-cyano-5-methanesulfonyl-thiophene-2-carboxylic acid ethyl ester gives the title compound.

출처 및 근거

ORD 기록
ord-961ec4031e5a487681f56ab476292091
출처 데이터셋
uspto-grants-2010_01
특허 번호
US07642361B2

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