반응식
Cl.[CH3:2][NH:3][CH2:4][CH2:5][CH2:6][C:7]([OH:9])=[O:8].S(Cl)(Cl)=O.[CH3:14]O>>[CH3:14][O:8][C:7](=[O:9])[CH2:6][CH2:5][CH2:4][NH:3][CH3:2]참가 물질
4
반응 조건
- 온도
- 0 °C
실험 절차
4-(methylamino) butyric acid HCl was dissolved in methanol and thionyl chloride in catalytic amount was added drop by drop. The reaction mixture was stirred at 0° C. for 30 min. Thereafter, the solvent was reduced in vacu, yielding a white solid.
후처리
- customyielding a white solid
출처 및 근거
- ORD 기록
- ord-a3dd38a54c534097bca325db7a81d19e
- 출처 데이터셋
- uspto-grants-2010_01
- 특허 번호
- US07645903B2
연결된 노트
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