4-Ethylphenyl isocyanate → HCID 58659386, 화합물

반응식

[NH2:1][C:2]1[CH:16]=[CH:15][C:5]([O:6][C:7]2[CH:12]=[CH:11][N:10]=[C:9]([O:13][CH3:14])[CH:8]=2)=[CH:4][CH:3]=1.[CH2:17]([C:19]1[CH:24]=[CH:23][C:22]([N:25]=[C:26]=[O:27])=[CH:21][CH:20]=1)[CH3:18]>>[CH3:14][O:13][C:9]1[CH:8]=[C:7]([O:6][C:5]2[CH:15]=[CH:16][C:2]([NH:1][C:26]([NH:25][C:22]3[CH:23]=[CH:24][C:19]([CH2:17][CH3:18])=[CH:20][CH:21]=3)=[O:27])=[CH:3][CH:4]=2)[CH:12]=[CH:11][N:10]=1

참가 물질

반응물 2

HCID 900074-Ethylphenyl isocyanate

HCID 68539011HCID 68539011, 화합물

생성물 1

HCID 58659386HCID 58659386, 화합물

실험 절차

The title compound is prepared from 4-(4-amino-phenoxy)-2-methoxy-pyridine (Stage 92.1; 91 mg, 0.42 mmol) and 4-ethyl-phenyl-isocyanate (124 μl, 0.84 mmol) analogously to Example 89: m.p.: 196° C.; Anal.: CHN.

출처 및 근거

ORD 기록: ord-cb69accd58e94a098a0c6af38868e8be
출처 데이터셋: uspto-grants-2010_01
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07652022B2

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