Selenium Dioxide → 6-Methoxyquinoline-2-carbaldehyde

HRID 1993787노트

반응식

[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[N:9]=[C:8]([CH3:13])[CH:7]=[CH:6]2.[Se](=O)=[O:15]>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[N:9]=[C:8]([CH:13]=[O:15])[CH:7]=[CH:6]2

참가 물질

반응물 2

HCID 24007Selenium Dioxide

HCID 706486-Methoxyquinaldine

생성물 1

HCID 15488726-Methoxyquinoline-2-carbaldehyde수율 68%

실험 절차

The title compound was prepared from 6-methoxy-2-methylquinoline (6g) and selenium dioxide using methods as described in the literature for similar compounds (Mathes et al., 1957) in 68% yield.

출처 및 근거

ORD 기록: ord-c6d9db08563e45c797ca38d16c1d0fe7
출처 데이터셋: uspto-grants-2010_01
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07652036B2

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