Thionyl Chloride → HCID 178428764, 화합물

HRID 1995362노트

반응식

HRID 1995362 반응식
[N+:1]([C:4]1[CH:9]=[C:8]([CH3:10])[N:7]=[C:6]([C:11]([OH:13])=O)[CH:5]=1)([O-:3])=[O:2].S(Cl)(Cl)=O.[NH2:18][C:19]1[NH:23][N:22]=[N:21][N:20]=1>>[NH:20]1[C:19]([NH:18][C:11]([C:6]2[CH:5]=[C:4]([N+:1]([O-:3])=[O:2])[CH:9]=[C:8]([CH3:10])[N:7]=2)=[O:13])=[N:23][N:22]=[N:21]1

참가 물질

4

반응물 3

HCID 24386Thionyl ChlorideHCID 112753916-methyl-4-nitropicolinic acidHCID 178509299HCID 178509299, 화합물

생성물 1

HCID 178428764HCID 178428764, 화합물수율 40.1%

실험 절차

1.44 g of 4-nitro-6-methyl-2-pyridinecarboxylic acid, 27 ml of thionyl chloride and 0.79 g of 5-aminotetrazole are treated in the same manner as described in Example 1. The crude product thus obtained is washed with ethanol, whereby 0.79 g of N-(5-tetrazolyl)-4-nitro-6-methyl-2-pyridinecarboxamide is obtained.

후처리

  1. customThe crude product thus obtained
  2. washis washed with ethanol

출처 및 근거

ORD 기록
ord-65871b5624ae49da81f39eef8fbc239d
출처 데이터셋
uspto-grants-1983_09
특허 번호
US04404214

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