Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pyridine → N-(chloroacetoxy)-3-chloro-N-(2-chlorophenyl)methyl-2,2-dimethylpropanamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pyridine | HCID 1049 | — |
| 반응물 | Chloroacetyl chloride | HCID 6577 | — |
| 반응물 | 3-chloro-N-(2-chlorophenyl)methyl-N-hydroxy-2,2-dimethylpropanamide | HCID 9925558 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | N-(chloroacetoxy)-3-chloro-N-(2-chlorophenyl)methyl-2,2-dimethylpropanamide | HCID 13192525 | — |
반응 단계
This compound was prepared in the manner of Example 13, using 4.0 g (0.014 mole) of 3-chloro-N-(2-chlorophenyl)methyl-N-hydroxy-2,2-dimethylpropanamide (prepared in Example 1), 1.6 g (0.014 mole) of chloroacetyl chloride, and 1.2 g (0.015 mole) of pyridine, in 50 ml toluene. The product was a liquid, of which nmr and ir spectra were consistent with the assigned structure.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04405357 |
| 출처 데이터셋 | uspto-grants-1983_09 |
| ORD ID | ord-9ad350d0eae44ae09e8fa8044bb1c917 |
| 출처 메모 | uspto-grants-1983_09 |