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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1995499생성일: 2026년 10월 25일

Sebacic Acid → Hexadecylketene

https://huagongshe.com/reaction/1995499

반응식

참여 물질

역할이름HCID투입량
반응물Sebacic AcidHCID 5192—
반응물TriethylenetetramineHCID 5565—
반응물EpichlorohydrinHCID 7835—
반응물PentaethylenehexamineHCID 19990—
반응물2-Hydroxystearic acidHCID 69417—
용매Acetic AcidHCID 176—
용매WaterHCID 962—
생성물HexadecylketeneHCID 23293311—

반응 단계

Except that 60.5 g of castor oil fatty acid, 20.2 g of sebacic acid and 48.7 g of pentaethylenehexamine were used instead of hydroxystearic acid and triethylenetetramine, the same procedures and conditions as those used in the foregoing Example 1 were repeated to subject the input materials to a reaction. At the end of the reaction, 54 g of glacial acetic acid was added thereto, followed by dilution with warm water. Then, after adding 7.4 g of epichlorohydrin thereto, the resultant system was subjected to a reaction at 80°-85° C. for 2 hours to produce a dispersion having a solid content of 20% by weight. Hereinafter, this dispersion shall be referred to as the dispersing agent Hs according to the present invention. Thereafter, by using 10 parts by weight, as solid content, of the dispersing agent Hs, a dispersion of hexadecyl ketene dimer was prepared in the same manner as in the preceding Example 7. Hereinafter, this dispersion shall be referred to as the cellulose treating agent H according to the present invention.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04405408
출처 데이터셋uspto-grants-1983_09
ORD IDord-81f598e6b96c4a75a2f9e9bc01822aee
출처 메모uspto-grants-1983_09