Ammonia → N-(2,4,6-tribromophenyl)glycinamide

HRID 1995760

반응식

HRID 1995760 반응식
[Br:1][C:2]1[CH:7]=[C:6]([Br:8])[CH:5]=[C:4]([Br:9])[C:3]=1NCC(OCC)=O.C1([NH:23][CH2:24][C:25](OCC)=[O:26])C=CC=CC=1.BrBr.[NH3:32]>O.C(O)(=O)C.C(O)C>[Br:1][C:2]1[CH:3]=[C:4]([Br:9])[CH:5]=[C:6]([Br:8])[C:7]=1[NH:32][C:25](=[O:26])[CH2:24][NH2:23]

참가 물질

8

반응물 4

HCID 222AmmoniaHCID 24408BromineHCID 75190N-Phenylglycine ethyl esterHCID 12659467ethyl N-(2,4,6-tribromophenyl)glycinate2회

생성물 1

HCID 28992175N-(2,4,6-tribromophenyl)glycinamide

시약·촉매·용매 3

HCID 176Acetic Acid용매HCID 702Ethanol용매HCID 962Water용매

실험 절차

The ester required for Id, ethyl N-(2,4,6-tribromophenyl)glycinate (IV), was prepared by the reaction of ethyl N-phenylglycinate with bromine in a mixture of water and acetic acid. IV reacted with ammonia is ethanol solution to form N-(2,4,6-tribromophenyl)glycinamide (V).

출처 및 근거

ORD 기록
ord-7571ebc6c3a74ab1bc12a27145db849d
출처 데이터셋
uspto-grants-1983_09
특허 번호
US04405806

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