Formaldehyde → HCID 20402431, 화합물
반응식
[CH:1]([NH:4][CH:5]([CH3:11])[CH2:6][O:7][CH:8]([OH:10])[CH3:9])([CH3:3])[CH3:2].[CH2:12]=O>[Pd].CO>[CH:1]([N:4]([CH:5]([CH3:11])[CH2:6][O:7][CH:8]([OH:10])[CH3:9])[CH3:12])([CH3:3])[CH3:2]참가 물질
5
반응 조건
- 온도
- 80 °C
실험 절차
A total of 155 g of 2-(isopropylamino) propoxyethanol, 122 g of 37% aqueous formaldehyde, 5 g of 10% Pd/C and 1 l of methanol were charged to an autoclave, pressured to 1000 psi with H2 and heated at 80° C. for 3 hours. Filtration and distillation of the reaction mixture yielded 159 g of 2-(N-isopropyl-N-methylamino)propoxyethanol with b.p. of 125° C. at 20 mm.
후처리
- filtrationFiltration and distillation of the reaction mixture
출처 및 근거
- ORD 기록
- ord-6e7945c5f7b24739a959cda60bcbe050
- 출처 데이터셋
- uspto-grants-1983_09
- 특허 번호
- US04405811
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