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llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
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{4-[(Undecyloxy)methyl]phenyl}methanol → 4-[(Undecyloxy)methyl]benzaldehyde

HRID 1995778
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인쇄 미리보기

반응식

HRID 1995778 반응식
[CH2:1]([O:12][CH2:13][C:14]1[CH:21]=[CH:20][C:17]([CH2:18][OH:19])=[CH:16][CH:15]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11].[Cr](Cl)([O-])(=O)=O.[NH+]1C=CC=CC=1>C(Cl)Cl>[CH2:1]([O:12][CH2:13][C:14]1[CH:15]=[CH:16][C:17]([CH:18]=[O:19])=[CH:20][CH:21]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 2

HCID 53860858{4-[(Undecyloxy)methyl]phenyl}methanolHCID 178418287HCID 178418287, 화합물

생성물 1

HCID 204880034-[(Undecyloxy)methyl]benzaldehyde

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

p-(n-Undecyloxymethyl)benzyl alcohol (10 mmoles) is dissolved in methylene chloride and treated with pyridinium chlorochromate (12 mmoles) at room temperature. When the reaction ceases, the reaction mixture is filtered through a pad of silica gel. The solvent is evaporated from this filtrate to afford the product, p-(n-undecyloxymethyl)benzaldehyde.

후처리

  1. customWhen the reaction ceases
  2. filtrationthe reaction mixture is filtered through a pad of silica gel
  3. customThe solvent is evaporated from this filtrate

출처 및 근거

ORD 기록
ord-c3ff4db647464e1d9a43e4bc6eb3dfcb
출처 데이터셋
uspto-grants-1983_09
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04405810

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