Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-(2-methoxy-5-nitrophenyl)methanesulfonamide → N-(5-amino-2-methoxyphenyl)methanesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-(2-methoxy-5-nitrophenyl)methanesulfonamide | HCID 743556 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | N-(5-amino-2-methoxyphenyl)methanesulfonamide | HCID 10775094 | — |
반응 단계
A solution of 2-Methoxy-5-nitro-methanesulfonylaminobenzene (1 g) in methanol (20 ml) containing palladium on carbon (10%, 100 mg) was stirred at RT under hydrogen for 48 h. The mixture was filtered through celite then evaporated to give 2-methoxy-5-amino-methanesulfonylaminobenzene as a brown gum. This was used without purification in the following reaction.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07745490B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-8b2221c0082a4c95abf5c3c40f2e6318 |
| 출처 메모 | uspto-grants-2010_06 |