Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethyl phosphite → 5-(Diethylphosphono)pentyl acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethyl phosphite | HCID 31215 | — |
| 반응물 | 5-Bromopentyl acetate | HCID 85140 | — |
| 생성물 | 5-(Diethylphosphono)pentyl acetate | HCID 19689222 | — |
반응 단계
100.34 g (0.48 mol) of 5-bromopentyl acetate were heated at 150° C. for 8 hours with 79.8 g (0.048 mol) of triethyl phosphite while stirring and passing in nitrogen. The mixture was then fractionally distilled under reduced pressure.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05728686 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-37e8c73db5a4451484b91a4dd3cc9bb3 |
| 출처 메모 | uspto-grants-1998_03 |