Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Carbonate → Diethyl 5-hydroxypentylphosphonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Carbonate | HCID 10340 | — |
| 반응물 | 5-(Diethylphosphono)pentyl acetate | HCID 19689222 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Diethyl 5-hydroxypentylphosphonate | HCID 10680635 | — |
반응 단계
92 g (0.345 mol) of 5-(diethylphosphono)pentyl acetate were heated at 50° C. for 10 hours with stirring with 74 g (0.7 mol) of finely powdered sodium carbonate in 500 ml of methanol. The solution was filtered, concentrated and distilled in a bulb tube.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05728686 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-c88ff47b784b42e596807b91fc6e4cda |
| 출처 메모 | uspto-grants-1998_03 |