3-(3-Chlorophenyl)-2-propynal → 3-(3-Chlorophenyl)prop-2-ynal oxime

HRID 2040862노트

반응식

HRID 2040862 반응식
[C:1]1([C:7]#[C:8][CH:9]=[N:10][OH:11])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Cl:12]C1C=C(C#CC=O)C=CC=1>>[Cl:12][C:3]1[CH:2]=[C:1]([C:7]#[C:8][CH:9]=[N:10][OH:11])[CH:6]=[CH:5][CH:4]=1

참가 물질

3

반응물 2

HCID 468725403-(3-Chlorophenyl)-2-propynalHCID 765430553-Phenylprop-2-ynal oxime

생성물 1

HCID 765430563-(3-Chlorophenyl)prop-2-ynal oxime수율 96.4%

실험 절차

The title compound was prepared following the method here described for Compound 1a, using Compound 31d instead of phenylpropiolaldehyde. The pale brown residue was used in the next step without further purification. Yield: 96.4%.

후처리

  1. customThe pale brown residue was used in the next step without further purification

출처 및 근거

ORD 기록
ord-a3b51d3f27f14f879e822be58fb81423
출처 데이터셋
uspto-grants-2013_11
특허 번호
US08580962B2

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