1-(3,3-Diethoxyprop-1-yn-1-yl)-3-methylbenzene → 3-(m-Tolyl)propiolaldehyde

반응식

ClC1C=C(C#CC=O)C=CC=1.C([O:14][CH:15](OCC)[C:16]#[C:17][C:18]1[CH:23]=[CH:22][CH:21]=[C:20]([CH3:24])[CH:19]=1)C>>[CH3:24][C:20]1[CH:19]=[C:18]([C:17]#[C:16][CH:15]=[O:14])[CH:23]=[CH:22][CH:21]=1

참가 물질

반응물 2

HCID 107988731-(3,3-Diethoxyprop-1-yn-1-yl)-3-methylbenzene

HCID 468725403-(3-Chlorophenyl)-2-propynal

생성물 1

HCID 107731013-(m-Tolyl)propiolaldehyde

실험 절차

The title compound was synthesized following the procedure reported for Compound 31d, but starting from Compound 91a instead of Compound 31c. The crude title compound was used in the next step without further purification.

후처리

customThe crude title compound was used in the next step without further purification

출처 및 근거

ORD 기록: ord-0ac243aaa1b841659bffd022b0fab313
출처 데이터셋: uspto-grants-2013_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08580962B2

반응 노트

불러오는 중…