3-(m-Tolyl)propiolaldehyde → N-hydroxy-3-(3-methylphenyl)prop-2-yn-1-imine

HRID 2040888노트

반응식

HRID 2040888 반응식
Cl[C:2]1[CH:3]=[C:4]([C:8]#[C:9][CH:10]=[N:11][OH:12])[CH:5]=[CH:6][CH:7]=1.[CH3:13]C1C=C(C#CC=O)C=CC=1>>[OH:12][N:11]=[CH:10][C:9]#[C:8][C:4]1[CH:5]=[CH:6][CH:7]=[C:2]([CH3:13])[CH:3]=1

참가 물질

3

반응물 2

HCID 107731013-(m-Tolyl)propiolaldehydeHCID 765430563-(3-Chlorophenyl)prop-2-ynal oxime

생성물 1

HCID 86662876N-hydroxy-3-(3-methylphenyl)prop-2-yn-1-imine

실험 절차

The title compound was synthesized following the procedure reported for Compound 31e but starting from Compound 91b instead of Compound 31d. The crude title compound (brownish oil) was used in the next step without further purification.

후처리

  1. customThe crude title compound (brownish oil) was used in the next step without further purification

출처 및 근거

ORD 기록
ord-740331082d32413fb3a8b9f2ace8b25a
출처 데이터셋
uspto-grants-2013_11
특허 번호
US08580962B2

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