Aniline → N-phenyl-2-Dibenzofuranamine

HRID 2040943

반응식

HRID 2040943 반응식
I[C:2]1[CH:14]=[CH:13][C:5]2[O:6][C:7]3[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=3[C:4]=2[CH:3]=1.[NH2:15][C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1.C(OCC)(=O)C>CCCCCC>[CH:3]1[C:4]2[C:8]3[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=3[O:6][C:5]=2[CH:13]=[CH:14][C:2]=1[NH:15][C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1

참가 물질

5

반응물 3

HCID 6115AnilineHCID 8857Ethyl AcetateHCID 2233272-Iododibenzofuran

생성물 1

HCID 67204676N-phenyl-2-Dibenzofuranamine

시약·촉매·용매 1

HCID 8058Hexane용매

실험 절차

The Rf values of the objective substance, 2-iododibenzofuran, and aniline were respectively 0.28, 0.59, and 0.07, which were found by silica gel thin layer chromatography (TLC) (with a developing solvent of ethyl acetate and hexane in a ratio of 1:10).

출처 및 근거

ORD 기록
ord-4184c7be028a4bc1bb941d5e1b8ce571
출처 데이터셋
uspto-grants-2013_11
특허 번호
US08580980B2

연결된 노트

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