3-Methylphenylacetylene → HCID 53245751, 화합물

반응식

Br[C:2]1[CH:3]=[N:4][C:5]2[N:6]([N:8]=[C:9]([N:11]3[CH2:16][CH2:15][O:14][CH2:13][CH2:12]3)[N:10]=2)[CH:7]=1.[C:17]([C:19]1[CH:24]=[CH:23][CH:22]=[C:21]([CH3:25])[CH:20]=1)#[CH:18]>>[N:11]1([C:9]2[N:10]=[C:5]3[N:4]=[CH:3][C:2]([C:18]#[C:17][C:19]4[CH:20]=[C:21]([CH3:25])[CH:22]=[CH:23][CH:24]=4)=[CH:7][N:6]3[N:8]=2)[CH2:16][CH2:15][O:14][CH2:13][CH2:12]1

참가 물질

반응물 2

HCID 1366003-Methylphenylacetylene

HCID 58316703HCID 58316703, 화합물

생성물 1

HCID 53245751HCID 53245751, 화합물

실험 절차

The title compound, a brown solid, MS: m/e=320.2 (M+H+), can be prepared in accordance with the general method of example 1 from 6-bromo-2-morpholin-4-yl-[1,2,4]triazolo[1,5-a]pyrimidine (example 47, step 1) and ethynyl-3-methylbenzene.

출처 및 근거

ORD 기록: ord-ad6743f0324c425b8135494ffeb8f5b2
출처 데이터셋: uspto-grants-2013_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08586581B2

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