1,1'-Thiocarbonyldi-2(1H)-pyridone → N-(2,4-Dichloro-3-isothiocyanato-benzyl)-1-trifluoromethyl-cyclopropane carboxamide

HRID 2042804

반응식

HRID 2042804 반응식
[Cl:1][C:2]1[C:18]([NH2:19])=[C:17]([Cl:20])[CH:16]=[CH:15][C:3]=1[CH2:4][NH:5][C:6]([C:8]1([C:11]([F:14])([F:13])[F:12])[CH2:10][CH2:9]1)=[O:7].[C:21](N1C=CC=CC1=O)(N1C=CC=CC1=O)=[S:22]>>[Cl:1][C:2]1[C:18]([N:19]=[C:21]=[S:22])=[C:17]([Cl:20])[CH:16]=[CH:15][C:3]=1[CH2:4][NH:5][C:6]([C:8]1([C:11]([F:13])([F:14])[F:12])[CH2:10][CH2:9]1)=[O:7]

참가 물질

3

반응물 2

HCID 8531621,1'-Thiocarbonyldi-2(1H)-pyridoneHCID 56839976N-(2,4-Dichloro-3-amino-benzyl)-1-trifluoromethyl-cyclopropane carboxamide

생성물 1

HCID 56840197N-(2,4-Dichloro-3-isothiocyanato-benzyl)-1-trifluoromethyl-cyclopropane carboxamide

실험 절차

The title compound is prepared from N-(2,4-dichloro-3-amino-benzyl)-1-trifluoromethyl-cyclopropane carboxamide (150 mg, 0.45 mmol) and 1,1′-thiocarbonyldi-2-pyridone (89 mg, 0.38 mmol) in analogy to example Af.

출처 및 근거

ORD 기록
ord-a1f36131017c4b5bb9891572c7ddb579
출처 데이터셋
uspto-grants-2013_11
특허 번호
US08586604B2

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