Phosphine oxide, (chloromethyl)dimethyl- → HCID 19689185, 화합물

HRID 2044

반응식

HRID 2044 반응식
[Na].[Na].[CH3:3][N:4]1[C:12]2[N:11]=[CH:10][NH:9][C:8]=2[C:7](=[O:13])[NH:6][C:5]1=[O:14].Cl[CH2:16][P:17](=[O:20])([CH3:19])[CH3:18]>>[CH3:16][P:17]([CH3:18])([N:9]1[C:8]2[C:7](=[O:13])[N:6]([CH2:16][P:17](=[O:20])([CH3:19])[CH3:18])[C:5](=[O:14])[N:4]([CH3:3])[C:12]=2[N:11]=[CH:10]1)=[O:20]

참가 물질

3

반응물 2

HCID 74224Phosphine oxide, (chloromethyl)dimethyl-HCID 68880016HCID 68880016, 화합물

생성물 1

HCID 19689185HCID 19689185, 화합물

실험 절차

The title substance was prepared from 22 g (0.1 mol) of 3-methylxanthine disodium salt and chloromethyldimethylphosphine oxide analogously to Example 59 and crystallized from methanol.

후처리

  1. customcrystallized from methanol

출처 및 근거

ORD 기록
ord-c44c4a79058347d5a7012c9e47dfad0e
출처 데이터셋
uspto-grants-1998_03
특허 번호
US05728686

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