Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanone, 2-chloro-1,2-diphenyl- → Thiazole, triphenyl-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanone, 2-chloro-1,2-diphenyl- | HCID 95343 | — |
| 반응물 | Thiobenzamide | HCID 683563 | — |
| 용매 | Isopropanol | HCID 3776 | — |
| 생성물 | Thiazole, triphenyl- | HCID 1712256 | — |
반응 단계
Thiobenzamide (13.7 g, 0.10 mole) and desyl chloride (23.1 g, 0.10 mole) are heated under reflux in isopropyl alcohol (100 ml) for three hours. When the reaction mixture is cooled, the white solid precipitate formed is filtered off, washed twice with isopropyl alcohol, and dried. The yield of triphenylthiazole, m.p. 84°-85.5° C., is 21.5 g or 69%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04197306 |
| 출처 데이터셋 | uspto-grants-1980_04 |
| ORD ID | ord-3912ad2349f94687be5fa180fdf6869a |
| 출처 메모 | uspto-grants-1980_04 |