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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2049272생성일: 2026년 10월 27일

Ethanone, 2-chloro-1,2-diphenyl- → Thiazole, triphenyl-

https://huagongshe.com/reaction/2049272

반응식

참여 물질

역할이름HCID투입량
반응물Ethanone, 2-chloro-1,2-diphenyl-HCID 95343—
반응물ThiobenzamideHCID 683563—
용매IsopropanolHCID 3776—
생성물Thiazole, triphenyl-HCID 1712256—

반응 단계

Thiobenzamide (13.7 g, 0.10 mole) and desyl chloride (23.1 g, 0.10 mole) are heated under reflux in isopropyl alcohol (100 ml) for three hours. When the reaction mixture is cooled, the white solid precipitate formed is filtered off, washed twice with isopropyl alcohol, and dried. The yield of triphenylthiazole, m.p. 84°-85.5° C., is 21.5 g or 69%.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04197306
출처 데이터셋uspto-grants-1980_04
ORD IDord-3912ad2349f94687be5fa180fdf6869a
출처 메모uspto-grants-1980_04