Chloride → (2-Thienyl) (2,3-dimethyl-4-methoxyphenyl)ketone

HRID 2049304노트

반응식

HRID 2049304 반응식
[Cl-].[S:2]1[CH:6]=[CH:5][CH:4]=[C:3]1[C:7]([OH:9])=O.[CH3:10][C:11]1[C:16]([CH3:17])=[CH:15][CH:14]=[CH:13][C:12]=1[O:18][CH3:19]>>[S:2]1[CH:6]=[CH:5][CH:4]=[C:3]1[C:7]([C:15]1[CH:14]=[CH:13][C:12]([O:18][CH3:19])=[C:11]([CH3:10])[C:16]=1[CH3:17])=[O:9]

참가 물질

4

반응물 3

HCID 312ChlorideHCID 107002-Thiophenecarboxylic acidHCID 762692,3-Dimethylanisole

생성물 1

HCID 57091683(2-Thienyl) (2,3-dimethyl-4-methoxyphenyl)ketone수율 86%

실험 절차

This compound was prepared in 86% yield by using step (A) of Example 1 with the chloride of 2-thiophene carboxylic acid and 2,3-dimethyl anisole.

후처리

  1. customThis compound was prepared in 86% yield

출처 및 근거

ORD 기록
ord-1273e75270124de9a3250c1f7c36a043
출처 데이터셋
uspto-grants-1980_04
특허 번호
US04197309

반응 노트

불러오는 중…