Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzaldehyde → Benzaldehyde-4-chlorophenylnitrone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzaldehyde | HCID 240 | — |
| 반응물 | 4-Chlorophenylhydroxylamine | HCID 69983 | — |
| 반응물 | HCID 178526349 | HCID 178526349 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Benzaldehyde-4-chlorophenylnitrone | HCID 275545 | — |
반응 단계
p-Chlorophenylhydroxylamine (0.05 moles) was dissolved in warm 95% ethanol (20 cc) and was treated with benzaldehyde (0.05 moles) with vigorous stirring. The solid which formed was collected, washed with 95% ethanol, and recrystallized from ethanol to give 512 g. of α-phenyl-N-chlorophenylnitrone (m.p. 179°-82°).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04197314 |
| 출처 데이터셋 | uspto-grants-1980_04 |
| ORD ID | ord-f7ab9b2b911f437d895c72f75825324f |
| 출처 메모 | uspto-grants-1980_04 |