Ethanol → HCID 20344096, 화합물

HRID 2049628노트

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HRID 2049628 반응식
[F:1][C:2]1[CH:3]=[C:4]([CH:15]=[CH:16][CH:17]=1)[O:5][C:6]1[CH:14]=[CH:13][CH:12]=[CH:11][C:7]=1[C:8]([OH:10])=[O:9].OS(O)(=O)=O.[CH2:23](O)[CH3:24]>>[F:1][C:2]1[CH:3]=[C:4]([CH:15]=[CH:16][CH:17]=1)[O:5][C:6]1[CH:14]=[CH:13][CH:12]=[CH:11][C:7]=1[C:8]([O:10][CH2:23][CH3:24])=[O:9]

참가 물질

4

반응물 3

HCID 702EthanolHCID 1118Sulfuric AcidHCID 203440992-(3-Fluorophenoxy)benzoic acid

생성물 1

HCID 20344096HCID 20344096, 화합물

실험 절차

2-(3-Fluorophenoxy)benzoic acid (10 g.) and 100 ml of ethanol containing 1 ml. of concentrated H2SO4 were heated at reflux through molecular sieves overnight. The solvent was evaporated, and the residue poured into 50 ml. of 7% NaHCO3. The resulting ester was extracted with ether. ##STR10##

후처리

  1. temperatureat reflux through molecular sieves overnight
  2. customThe solvent was evaporated
  3. additionthe residue poured into 50 ml
  4. extractionThe resulting ester was extracted with ether

출처 및 근거

ORD 기록
ord-34832fdf8e0e476fa5110ec0262fc185
출처 데이터셋
uspto-grants-1980_04
특허 번호
US04198421

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