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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2049693생성일: 2026년 10월 26일

Flufenamic Acid → Ufenamate

https://huagongshe.com/reaction/2049693

반응식

참여 물질

역할이름HCID투입량
반응물Flufenamic AcidHCID 3371—
반응물Butyl bromideHCID 8002—
반응물PotassiumHCID 5462222—
용매DimethylformamideHCID 6228—
생성물UfenamateHCID 5632—

반응 단계

In anhydrous dimethyl formamide was dissolved 3.2 g. of potassium salt of N-(3-trifluoromethylphenyl)anthranilic acid. To the solution was added 5.0 g. of n-butyl bromide. The mixture was heated at 100°-120° C. for 5 hrs. while stirring. The precipitated potassium bromide was taken out by filtration. The filtrate was concentrated and the residue obtained was distilled to obtain 3.1 g. of light yellow liquid having a boiling point of 190°-192° C. (5 mmHg).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04198431
출처 데이터셋uspto-grants-1980_04
ORD IDord-c354eda409e54bc2b52759f93ba028d1
출처 메모uspto-grants-1980_04