Diethylamine → (Z,E)-N,N-diethyl-8-hydroxy-3,7-dimethyl-2,6-octadienamide
반응식
[OH:1][CH2:2]/[C:3](/[CH3:13])=[CH:4]/[CH2:5][CH2:6]/[C:7](/[CH3:12])=[CH:8]\[C:9]([OH:11])=O.[CH2:14]([N:16](CC)[CH2:17][CH3:18])[CH3:15].C(Cl)(=O)OCC.C(NCC)C>ClCCl>[CH2:14]([N:16]([CH2:17][CH3:18])[C:9](=[O:11])/[CH:8]=[C:7](/[CH3:12])\[CH2:6][CH2:5]/[CH:4]=[C:3](\[CH3:13])/[CH2:2][OH:1])[CH3:15]참가 물질
6
실험 절차
Following the same manner as in Example 5, the reaction and after-treatment were conducted by using 1.0 g of (E,E) and (Z,E)-8-hydroxy-3,7-dimethyl-2,6-octadienoic acid, 0.9 ml of triethylamine, 0.62 ml of ethyl chlorocarbonate and 0.67 ml of diethylamine in 20 ml of dichloromethane to afford 850 mg of the end product.
후처리
- customthe reaction
출처 및 근거
- ORD 기록
- ord-2a774a9cf6674827af4f87e0fd45025b
- 출처 데이터셋
- uspto-grants-1980_04
- 특허 번호
- US04199519
반응 노트
불러오는 중…