Hexane → HCID 12477037, 화합물
반응식
[S:1]1(=[O:7])[CH:5]=[CH:4][C:3](=[O:6])[NH:2]1.[CH3:8][C:9]([C:11]([CH3:13])=[CH2:12])=[CH2:10].CCCCCC>C(Cl)CCl>[CH3:8][C:9]1[CH2:10][CH:4]2[C:3](=[O:6])[NH:2][S:1](=[O:7])[CH:5]2[CH2:12][C:11]=1[CH3:13]참가 물질
5
반응 조건
- 온도
- 60 °C
실험 절차
To a solution of 2.2 g (0.02 mole) of 4-isothiazolin-3-one 1-oxide in 50 ml of ethylene dichloride is added 2.0 g (0.024 mole) of 2,3-dimethyl-1,3-butadiene. The mixture is stirred and maintained at 60° C. overnight. Concentration of the mixture yields a thick oil, which affords a white solid on trituration with hexane. The solid is filtered and air dried to yield 3.4 g (90%) or product, m.p. 135°-137° C. which can be recrystallized from ethyl acetate-hexane.
후처리
- customConcentration of the mixture yields a thick oil, which
- filtrationThe solid is filtered
- customair dried
- customto yield 3.4 g (90%) or product, m.p. 135°-137° C. which
- customcan be recrystallized from ethyl acetate-hexane
출처 및 근거
- ORD 기록
- ord-d3a348bc5442424bafe618d95658cc3d
- 출처 데이터셋
- uspto-grants-1980_04
- 특허 번호
- US04199591
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