HCID 4763834, 화합물 → HCID 4764068, 화합물
반응식
[N+:1]([C:4]1[CH:17]=[CH:16][C:7]([NH:8][C:9]2[CH:10]=[C:11]([OH:15])[CH:12]=[CH:13][CH:14]=2)=[CH:6][CH:5]=1)([O-])=O>[C].[Pd]>[NH2:1][C:4]1[CH:17]=[CH:16][C:7]([NH:8][C:9]2[CH:10]=[C:11]([OH:15])[CH:12]=[CH:13][CH:14]=2)=[CH:6][CH:5]=1참가 물질
3
실험 절차
20 Grams of 3-(4-nitroanilino)phenol was reduced under ordinary pressure in alcohol by the use of a palladium-carbon catalyst. After removing the catalyst by filtration, the alcohol was distilled off under reduced pressure and the residual solids were washed with benzene. The yield was 14 g, and melting point was 146°-149° C.
후처리
- customAfter removing the catalyst
- filtrationby filtration
- distillationthe alcohol was distilled off under reduced pressure
- washthe residual solids were washed with benzene
출처 및 근거
- ORD 기록
- ord-19510d727cd942f7830f05a204fe6628
- 출처 데이터셋
- uspto-grants-1980_04
- 특허 번호
- US04200466
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