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Water → HCID 20341782, 화합물

HRID 2050128
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HRID 2050128 반응식
[NH2:1][C:2]1[CH:15]=[CH:14][C:5]([NH:6][C:7]2[CH:8]=[C:9]([OH:13])[CH:10]=[CH:11][CH:12]=2)=[CH:4][CH:3]=1.C([O-])(=O)C.[Na+].[C:21]([C:26]1[CH:36]=[C:35]([C:37]([CH2:40][CH3:41])([CH3:39])[CH3:38])[CH:34]=[CH:33][C:27]=1[O:28][CH2:29][C:30](Cl)=[O:31])([CH2:24][CH3:25])([CH3:23])[CH3:22].O>C(O)(=O)C>[C:21]([C:26]1[CH:36]=[C:35]([C:37]([CH2:40][CH3:41])([CH3:39])[CH3:38])[CH:34]=[CH:33][C:27]=1[O:28][CH2:29][C:30]([NH:1][C:2]1[CH:15]=[CH:14][C:5]([NH:6][C:7]2[CH:8]=[C:9]([OH:13])[CH:10]=[CH:11][CH:12]=2)=[CH:4][CH:3]=1)=[O:31])([CH2:24][CH3:25])([CH3:23])[CH3:22]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

6

반응물 4

HCID 962WaterHCID 66612(2,4-Bis(1,1-dimethylpropyl)phenoxy)acetyl chlorideHCID 517045Sodium AcetateHCID 4764068HCID 4764068, 화합물

생성물 1

HCID 20341782HCID 20341782, 화합물

시약·촉매·용매 1

HCID 176Acetic Acid용매

실험 절차

To a solution of 11 g (0.055 mol) of 3-(4-aminoanilino)phenol in glacial acetic acid was added 4.6 g of anhydrous sodium acetate. During agitation at room temperature, the mixture was charged with 17.1 g (0.055 mol) of 2,4-di-tert-amylphenoxyacetyl chloride at a temperature below 30° C. After continuing the agitation for an additional 30 minutes at that temperature, the mixture was poured into iced water, and the deposited crystals were filtered, followed by recrystallization with methanol. The yield was 20 g and the melting point was 150°-152° C.

후처리

  1. customfor an additional 30 minutes
  2. filtrationthe deposited crystals were filtered
  3. customfollowed by recrystallization with methanol

출처 및 근거

ORD 기록
ord-940984dad9cf4877a7cd622a5837b788
출처 데이터셋
uspto-grants-1980_04
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04200466

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