Phenoxyethanol → 2-phenoxyethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate

HRID 2050811

반응식

HRID 2050811 반응식
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16]#[N:17])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[O:18]([CH2:25][CH2:26][OH:27])[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:17])[O:27][CH2:26][CH2:25][O:18][C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1

참가 물질

3

반응물 2

HCID 31236PhenoxyethanolHCID 198338865,7-dihydro-6H-dibenz[c,e]azepine-6carbonitrile

생성물 1

HCID 198339622-phenoxyethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate

실험 절차

starting from 5,7-dihydro-6H-dibenz[c,e]azepine-6-carbonitrile and 2-phenoxyethanol, there is obtained 2-phenoxyethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate as a resin, mass spectrum m/e: M+ 358 (20), 265 (7), 237 (65), 194 (100);

출처 및 근거

ORD 기록
ord-dc69df93f9e34a438d677d4ee10bda32
출처 데이터셋
uspto-grants-1991_05
특허 번호
US05015640

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